2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

Base Information

Chemical Name:2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester
CAS No.:135388-95-3
Molecular Formula:C₂₆H₂₇NO₇
Molecular Weight:465.503
Hs Code.:

Synonyms:2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

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Chemical Property of 2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

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Technology Process of 2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

There total 3 articles about 2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 64-17-5
ethanol

: 135388-94-2
3-Benzyloxy-2-methoxy-2'-nitrodiphenylether-4',5-dicarbonsaeuredimethylester

: 135388-95-3
2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

Guidance literature:: With hydrogenchloride; tin(ll) chloride; at 20 ℃; for 12h;
DOI:10.1055/s-1991-26496

Reference yield:

: 14719-83-6
methyl 3-nitro-4-chlorobenzoate

: 135388-95-3
2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 20 deg C, 15 min 2.) 125 deg C, 45 min

2: 70 percent / SnCl₂, HCl / 12 h / 20 °C

With hydrogenchloride; sodium hydride; tin(ll) chloride;
DOI:10.1055/s-1991-26496

Reference yield:

: 135388-93-1
5-Benzyloxy-3-hydroxy-4-methoxybenzoesaeuremethylester

: 135388-95-3
2'-Amino-3-benzyloxy-2-methoxydiphenylether-4',5-dicarbonsaeurediethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) DMF, 20 deg C, 15 min 2.) 125 deg C, 45 min

2: 70 percent / SnCl₂, HCl / 12 h / 20 °C

With hydrogenchloride; sodium hydride; tin(ll) chloride;
DOI:10.1055/s-1991-26496