(2-(Dimethylamino)ethyl)triphenylphosphonium bromide

Base Information

• Chemical Name: (2-(Dimethylamino)ethyl)triphenylphosphonium bromide
• CAS No.: 21331-80-6
• Molecular Formula: C22H25 N P . Br
• Molecular Weight: 414.325
• Hs Code.: 2931900090
• European Community (EC) Number: 244-335-2
• DSSTox Substance ID: DTXSID30943890
• Mol file: 21331-80-6.mol

Synonyms:21331-80-6;(2-(Dimethylamino)ethyl)triphenylphosphonium bromide;(2-Dimethylaminoethyl)triphenylphosphonium bromide;2-Dimethylaminoethyltriphenylphosphonium Bromide;2-(dimethylamino)ethyl-triphenylphosphanium;bromide;[2-(dimethylamino)ethyl]triphenylphosphonium bromide;EINECS 244-335-2;SCHEMBL143506;DTXSID30943890;YIIHEMGEQQWSMA-UHFFFAOYSA-M;MFCD00011794;AKOS015833079;CS-0324002;D1654;FT-0605397;triphenyldimethylaminoethylphosphonium bromide;D89901;2-dimethylaminoethyl triphenylphosphonium bromide;N,N-Dimethylaminoethyltriphenylphosphonium bromide;(2-dimethylaminoethyl)triphenyl phosphonium bromide;2-(dimethylamino)ethyl-triphenylphosphonium bromide;A815278;2-(dimethylamino)ethyl-triphenyl-phosphanium bromide;J-013999;(2-(dimethylamino)ethyl)-triphenylphosphonium bromide;[2-(Dimethylamino)ethyl](triphenyl)phosphanium bromide;[2-(dimethylamino)ethyl](triphenyl)phosphonium bromide

Chemical Property of (2-(Dimethylamino)ethyl)triphenylphosphonium bromide

Chemical Property:

• Appearance/Colour: yellow powder
• Melting Point: 195-200 °C (dec.)(lit.)
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 16.83000
• Density: g/cm³
• LogP: 0.54610
• Storage Temp.: Inert atmosphere,Room Temperature
• Sensitive.: Hygroscopic
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 6
• Exact Mass: 413.09080
• Heavy Atom Count: 25
• Complexity: 303

Purity/Quality:

97% ^*data from raw suppliers

2-Dimethylaminoethyltriphenylphosphonium Bromide ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CN(C)CC[P+](C1=CC=CC=C1)(C2=CC=CC=C2)C3=CC=CC=C3.[Br-]
• Uses: [2-(Dimethylamino)ethyl]triphenylphosphonium Bromide, can be used as a polymerizable cationic surfactant for the intercalation of montmorillonite (MMT), used in the synthesis of polystyrene-clay nanocomposite materials. It can also be used for the synthesis of some analogs of morphine 6-glucuronide through Wittig reactions.

Technology Process of (2-(Dimethylamino)ethyl)triphenylphosphonium bromide

There total 3 articles about (2-(Dimethylamino)ethyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2-methoxyethyl)triphenylphosphonium bromide (55894-16-1) + dimethyl amine (124-40-3) → [2-(dimethylamino)ethyl]triphenylphosphonium bromide (21331-80-6)

Guidance literature:

In methanol; water; at 80 ℃; for 18h;

DOI:10.1021/ml5000228

Reference yield: 60.0%

2-(N,N-dimethylamino)ethanol (108-01-0) + triphenylphosphine (603-35-0) → [2-(dimethylamino)ethyl]triphenylphosphonium bromide (21331-80-6)

Guidance literature:

With hydrogen bromide; In benzene; at 155 ℃; for 5h;

Reference yield:

→ [2-(dimethylamino)ethyl]triphenylphosphonium bromide (21331-80-6)

Guidance literature:

DOI:10.1002/hlca.19780610519

upstream raw materials:

2-(N,N-dimethylamino)ethanol

triphenylphosphine

(2-methoxyethyl)triphenylphosphonium bromide

dimethyl amine

Downstream raw materials:

[(dimethylamino)ethyl]triphenylphosphonium bromide

{6-[4-(3-dimethylamino-propenyl)-5-ethyl-2-methoxy-phenyl]-pyridin-2-yl}-carbamic acid tert-butyl ester

(2Z)-2-[14-cyclohexyl-11-(methoxycarbonyl)-6H-indolo[1,2-e][1,5]benzoxazocin-7(8H)-ylidene]-N,N-dimethylethanaminium trifluoroacetate