2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

Base Information

Chemical Name:2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline
CAS No.:1450665-95-8
Molecular Formula:C₄₇H₃₉N₃O₄
Molecular Weight:709.844
Hs Code.:

Synonyms:2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

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Chemical Property of 2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

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Technology Process of 2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

There total 1 articles about 2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1196061-68-3
2,9-bis(2,6-dimethoxyphenyl)-3-ethynyl-[1,10]-phenanthroline

: 1255535-41-1
4-((4-iodo-2,3,5,6-tetramethylphenyl)ethynyl)pyridine

: 1450665-95-8
2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 24h; Inert atmosphere;
DOI:10.1039/c3ob41258j

Reference yield: 100.0%

: 1450665-97-0
4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine

: 1450665-95-8
2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

: 54010-75-2
zinc trifluoromethanesulfonate

: 107-06-2,52399-93-6
1,2-dichloro-ethane

: C₇₅H₅₇N₇O₄Zn⁽²⁺⁾*2CF₃O₃S^(1-)*2.25C₂H₄Cl₂

Guidance literature:: In acetonitrile; for 2h; Reflux;
DOI:10.1039/c3ob41258j

Reference yield: 100.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 75-09-2
dichloromethane

: 1450665-97-0
4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine

: 1450665-98-1
3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

: 1450665-95-8
2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

: 54010-75-2
zinc trifluoromethanesulfonate

: C₁₅₅H₁₃₃Br₂Cu₂N₁₁O₆Zn⁽⁴⁺⁾*2F₆P^(1-)*2CF₃O₃S^(1-)*1.3CH₂Cl₂

Guidance literature:: dichloromethane; 4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine; 2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline; zinc trifluoromethanesulfonate; In acetonitrile; for 2h; Reflux;

tetrakis(actonitrile)copper(I) hexafluorophosphate; 3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline); for 1h; Reflux;
DOI:10.1039/c3ob41258j