3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

Base Information

Chemical Name:3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)
CAS No.:1450665-98-1
Molecular Formula:C₈₀H₇₆Br₂N₄O₂
Molecular Weight:1285.32
Hs Code.:

Synonyms:3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

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Chemical Property of 3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

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Technology Process of 3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

There total 1 articles about 3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 145483-70-1
1,4-di-n-butoxy-2,5-diiodobenzene

: 369390-72-7
2-(4-Bromo-2,3,5,6-tetramethylphenyl)-9-(2,4,6-trimethylphenyl)-3-ethynyl-[1,10]phenanthroline

: 1450665-98-1
3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In tetrahydrofuran; at 70 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c3ob41258j

Reference yield: 100.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 75-09-2
dichloromethane

: 1450665-97-0
4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine

: 1450665-98-1
3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline)

: 1450665-95-8
2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline

: 54010-75-2
zinc trifluoromethanesulfonate

: C₁₅₅H₁₃₃Br₂Cu₂N₁₁O₆Zn⁽⁴⁺⁾*2F₆P^(1-)*2CF₃O₃S^(1-)*1.3CH₂Cl₂

Guidance literature:: dichloromethane; 4'-(4-pyridin-4-ylethynyl-phenyl)[2,2';6',2'']terpyridine; 2,9-bis(2,6-dimethoxyphenyl)-3-((2,3,5,6-tetramethyl-4-(pyridin-4-ylethynyl)phenyl)ethynyl)-1,10-phenanthroline; zinc trifluoromethanesulfonate; In acetonitrile; for 2h; Reflux;

tetrakis(actonitrile)copper(I) hexafluorophosphate; 3,3'-(2,5-dibutoxy-1,4-phenylene)bis(ethyn-2,1-diyl)bis(2-(4-bromo-2,3,5,6-tetramethylphenyl)-9-mesityl-1,10-phenanthroline); for 1h; Reflux;
DOI:10.1039/c3ob41258j