2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

Base Information

Chemical Name:2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate
CAS No.:930110-23-9
Molecular Formula:C₁₉H₁₃Cl₃F₃NO₃
Molecular Weight:466.671
Hs Code.:

Synonyms:2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

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Chemical Property of 2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

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Technology Process of 2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

There total 6 articles about 2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67492-50-6
(3,5-dichlorophenyl)boronic acid

: 930110-23-9
2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran; water / 3 h / Heating / reflux

2.1: N-chloro-succinimide / 1,2-dimethoxyethane / 2 h / 70 °C

2.2: 20 h / 20 °C

3.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 3 h / 70 °C

4.1: acetic acid / 2 h / 120 °C

4.2: 20 °C

With N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; acetic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water; 1,2-dichloro-ethane;

Reference yield:

: 930110-20-6
3-(4-bromomethyl-3-chlorophenyl)-5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole

: 127-08-2
potassium acetate

: 930110-23-9
2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

Guidance literature:: 3-(4-bromomethyl-3-chlorophenyl)-5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazole; potassium acetate; With acetic acid; at 120 ℃; for 2h;

With water; sodium hydrogencarbonate; In chloroform; at 20 ℃;

Reference yield:

: 864725-22-4
1,3-dichloro-5-(3,3,3-trifluoroprop-1-en-2-yl)benzene

: 930110-23-9
2-chloro-4-[5-(3,5-dichlorophenyl)-5-trifluoromethyl-4,5-dihydroisoxazol-3-yl]benzyl acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-chloro-succinimide / 1,2-dimethoxyethane / 2 h / 70 °C

1.2: 20 h / 20 °C

2.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / 1,2-dichloro-ethane / 3 h / 70 °C

3.1: acetic acid / 2 h / 120 °C

3.2: 20 °C

With N-chloro-succinimide; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); acetic acid; In 1,2-dimethoxyethane; 1,2-dichloro-ethane;