Trimethylamine-N-ethylamidoborane

Base Information

Chemical Name:Trimethylamine-N-ethylamidoborane
CAS No.:60788-35-4
Molecular Formula:C6H15BN2O
Molecular Weight:144.023
Hs Code.:

Synonyms:Trimethylamine-N-ethylamidoborane;Boron, dihydro(N,N-dimethylmethanamine)((ethylamino)carbonyl)-, (T-4)-;SCHEMBL5474671;QCPYANBREBRQDF-UHFFFAOYSA-N;Trimethylamine (Ethylcarbamoyl)borane;NSC 337223;LS-44972

Suppliers and Price of Trimethylamine-N-ethylamidoborane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of Trimethylamine-N-ethylamidoborane

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:142.1277433
Heavy Atom Count:10
Complexity:62.8

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:[B]C(=O)NCC.CN(C)C

Technology Process of Trimethylamine-N-ethylamidoborane

There total 1 articles about Trimethylamine-N-ethylamidoborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 30353-61-8
trimethylamine-cyanoborane

: 368-39-8
triethyloxonium fluoroborate

: 60788-35-4
trimethylamine-(ethylcarbamoyl)borane

Guidance literature:: With sodium hydroxide; In sodium hydroxide; dichloromethane; soln. Me3N*BH2CN and Et3OBF4 in Ch2Cl2 refluxed under N2 for 24 h, mixt. cooled to 0°C and NaOH added slowly to pH 8 and mixt. stirred for 1 h at room temp.; org. layer separated and dried over MgSO4, solvent removed in vacuo, liquid distilled under vac. with min. heating; elem. anal.;

Reference yield: 77.7%

: 60788-35-4
trimethylamine-(ethylcarbamoyl)borane

: 124-40-3
dimethyl amine

: 88915-69-9
dimethylamine-(ethylcarbamoyl)borane

Guidance literature:: In neat (no solvent); anhyd. Me2NH cooled to 0°C and poured into vessel with Me3N*BH2CONHEt kept at 0°C, vessel kept at room temp. for 8.5 days with shaking; vessel cooled to 0°C and opened, pentane added, amine and solvent evapd., residue taken up in CH2Cl2 and washed with water, CH2Cl2 soln.dried over MgSO4 and treated with charcoal, solvent evapd., oil vac. distilled; elem. anal.;

Reference yield: 65.0%

: 60788-35-4
trimethylamine-(ethylcarbamoyl)borane

: 74-89-5
methylamine

: 88915-70-2
methylamine-(ethylcarbamoyl)borane

Guidance literature:: In neat (no solvent); anhyd. MeNH2 condensed at -78°C to pressure vessel with Me3N*BH2CONHEt cooled to -78°C and allowed to warm to room temp. and keptfor 1 week with shaking; vessel cooled to -78°C and opened, pentane added, excess amine allowed to evaporate at room temp., solvent evapd. in vacuo, product dissolved in CH2Cl2 and filtered into n-pentane, solid filtered; elem. anal.;