p-Chlorobenzyl Trifluoromethanesulfinate

Base Information

• Chemical Name: p-Chlorobenzyl Trifluoromethanesulfinate
• CAS No.: 130774-55-9
• Molecular Formula: C₈H₆ClF₃O₂S
• Molecular Weight: 258.649
• Mol file: 130774-55-9.mol

Synonyms:p-Chlorobenzyl Trifluoromethanesulfinate

Chemical Property of p-Chlorobenzyl Trifluoromethanesulfinate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of p-Chlorobenzyl Trifluoromethanesulfinate

There total 2 articles about p-Chlorobenzyl Trifluoromethanesulfinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

p-Chlorobenzyl Trifluoromethanesulfenate (66727-98-8) → p-Chlorobenzyl Trifluoromethanesulfinate (130774-55-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 0 ℃; for 2h;

Reference yield:

→ p-Chlorobenzyl Trifluoromethanesulfinate (130774-55-9)

Guidance literature:

entspr. Sulfenat ester, m-Chlorperbenzoesaeure;

Reference yield:

methanol (67-56-1) + p-Chlorobenzyl Trifluoromethanesulfinate (130774-55-9) → trifluoromethanesulfinic acid (34642-42-7) + 4-chlorobenzyl methyl ether (1195-44-4)

Guidance literature:

With 2,6-dimethylpyridine; at 32 ℃; Rate constant;

upstream raw materials:

p-Chlorobenzyl Trifluoromethanesulfenate

Downstream raw materials:

trifluoromethanesulfinic acid

4-chlorobenzyl methyl ether

1-chloro-4-(ethoxymethyl)benzene

Refernces