3',5'-DIFLUORO-2-PHENYLACETOPHENONE

Base Information

Chemical Name:3',5'-DIFLUORO-2-PHENYLACETOPHENONE
CAS No.:181697-20-1
Molecular Formula:C₁₄H₁₀F₂O
Molecular Weight:232.23
Hs Code.:
Mol file:181697-20-1.mol

Synonyms:1-(3,5-difluorophenyl)-2-phenylethanone

Suppliers and Price of 3',5'-DIFLUORO-2-PHENYLACETOPHENONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
3',5'-DIFLUORO-2-PHENYLACETOPHENONE
1g
$ 809.00

Rieke Metals
3',5'-DIFLUORO-2-PHENYLACETOPHENONE
5g
$ 1943.00

Crysdot
1-(3,5-Difluorophenyl)-2-phenylethanone 97%
25g
$ 3318.00

Crysdot
1-(3,5-Difluorophenyl)-2-phenylethanone 97%
10g
$ 1882.00

Crysdot
1-(3,5-Difluorophenyl)-2-phenylethanone 97%
5g
$ 1177.00

Crysdot
1-(3,5-Difluorophenyl)-2-phenylethanone 97%
1g
$ 437.00

Total 2 raw suppliers

Chemical Property of 3',5'-DIFLUORO-2-PHENYLACETOPHENONE

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

3',5'-DIFLUORO-2-PHENYLACETOPHENONE ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-36/37/39

MSDS Files:

Useful:

Technology Process of 3',5'-DIFLUORO-2-PHENYLACETOPHENONE

There total 4 articles about 3',5'-DIFLUORO-2-PHENYLACETOPHENONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 7677-24-9
trimethylsilyl cyanide

: 32085-88-4
3,5-difluorobenzaldehyde

: 100-39-0
benzyl bromide

: 181697-20-1
1-(3,5-difluorophenyl)-2-phenylethanone

Guidance literature:: With hydrogenchloride; sodium hydroxide; zinc diiodide; trifluoroacetic acid; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; dichloromethane; water;

Reference yield: 92.0%

: 32085-88-4
3,5-difluorobenzaldehyde

: 100-39-0
benzyl bromide

: 181697-20-1
1-(3,5-difluorophenyl)-2-phenylethanone

Guidance literature:: 3,5-difluorobenzaldehyde; With trimethylsilyl cyanide; zinc(II) iodide; In dichloromethane; at 0 ℃; for 16h;

With lithium diisopropyl amide; In tetrahydrofuran; n-heptane; ethylbenzene; at -78 - -60 ℃; for 0.5h;

benzyl bromide; With hydrogenchloride; trifluoroacetic acid; more than 3 stages;

Reference yield: 22.0%

: 103-82-2
phenylacetic acid

methyl 3,5-difluorobenzoate: 216393-55-4
methyl 3,5-difluorobenzoate

: 181697-20-1
1-(3,5-difluorophenyl)-2-phenylethanone

Guidance literature:: With lithium hexamethyldisilazane; In tetrahydrofuran; N,N-dimethyl-formamide; at -4 ℃; Inert atmosphere;
DOI:10.1021/acs.jmedchem.1c00235