N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

Base Information

Chemical Name:N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide
CAS No.:1313017-13-8
Molecular Formula:C₁₆H₂₂ClNO₂
Molecular Weight:295.809
Hs Code.:

Synonyms:N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

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Chemical Property of N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

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Technology Process of N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

There total 1 articles about N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 65854-91-3
N-(4-chlorophenyl)-2,2-dimethylpropionamide

: 3282-30-2
pivaloyl chloride

: 1313017-13-8
N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

Guidance literature:: N-(4-chlorophenyl)-2,2-dimethylpropionamide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; hexane; at -10 ℃; for 2h; Inert atmosphere;

pivaloyl chloride; In tetrahydrofuran; hexane; for 2h; Inert atmosphere;
DOI:10.1021/jo1025767

Reference yield: 94.0%

: 1313017-13-8
N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

: 581059-96-3
1-(2-amino-5-chlorophenyl)-2,2-dimethyl-1-propanone

Guidance literature:: With hydrogenchloride; water; at 90 ℃; for 12h;
DOI:10.1021/jo1025767

Reference yield: 86.0%

: 1313017-13-8
N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide

: 74-88-4
methyl iodide

: 1313017-14-9
N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-N,2,2-trimethylpropanamide

Guidance literature:: N-[4-chloro-2-(2,2-dimethyl-1-oxopropyl)phenyl]-2,2-dimethylpropanamide; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 1h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; for 5h;
DOI:10.1021/jo1025767