α,α-dimethoxy-4-fluorotoluene

Base Information

Chemical Name:α,α-dimethoxy-4-fluorotoluene
CAS No.:32691-93-3
Molecular Formula:C₉H₁₁FO₂
Molecular Weight:170.184
Hs Code.:

Synonyms:α,α-dimethoxy-4-fluorotoluene

Suppliers and Price of α,α-dimethoxy-4-fluorotoluene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of α,α-dimethoxy-4-fluorotoluene

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of α,α-dimethoxy-4-fluorotoluene

There total 3 articles about α,α-dimethoxy-4-fluorotoluene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 459-57-4
4-fluorobenzaldehyde

: 149-73-5
trimethyl orthoformate

: 32691-93-3
α,α-dimethoxy-4-fluorotoluene

Guidance literature:: With copper(II) bis(tetrafluoroborate); In methanol; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2005.09.168

Reference yield: 86.0%

: 67-56-1
methanol

: 405-99-2
para-fluorostyrene

: 32691-93-3
α,α-dimethoxy-4-fluorotoluene

Guidance literature:: With 2-Picolinic acid; ferrous(II) sulfate heptahydrate; dihydrogen peroxide; at 20 - 60 ℃; for 12h; Schlenk technique; Molecular sieve;
DOI:10.1002/cctc.201300270

Reference yield:

: 67-56-1
methanol

: 459-57-4
4-fluorobenzaldehyde

: 459-56-3
4-fluorobenzylic alcohol

: 32691-93-3
α,α-dimethoxy-4-fluorotoluene

Guidance literature:: With hydrogen; at 110 ℃; for 4h; under 7500.75 Torr; Overall yield = 98 percentChromat.; chemoselective reaction; Autoclave;
DOI:10.1002/cssc.201903123