benzoylcinchonine

Base Information

• Chemical Name: benzoylcinchonine
• CAS No.: 14402-57-4
• Molecular Formula: C₂₆H₂₆N₂O₂
• Molecular Weight: 398.505

Synonyms:benzoylcinchonine

Chemical Property of benzoylcinchonine

Chemical Property:

Purity/Quality:

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Technology Process of benzoylcinchonine

There total 5 articles about benzoylcinchonine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

sodium benzoate (532-32-1) + 2,2,2-trifluoroethanol (75-89-8) + methanesulfonic acid (quinolin-4-yl)(5-vinyl-1-azabicyclo[2.2.2]oct-2-yl)methyl ester (560119-43-9) → benzoylcinchonine (14402-57-4,1260207-33-7) + 4-[(S)-(2,2,2-Trifluoro-ethoxy)-((1S,2R,4S,5R)-5-vinyl-1-aza-bicyclo[2.2.2]oct-2-yl)-methyl]-quinoline + benzoic acid 2-(quinolin-4-yl)-6-vinyl-1-azabicyclo[3.2.2]non-3-yl-ester (560119-48-4)

Guidance literature:

for 4h; Heating;

DOI:10.1021/jo026890d

Reference yield: 54.0%

benzoic acid (65-85-0,8013-63-6) + Cinchonin (118-10-5) → benzoylcinchonine (14402-57-4,1260207-33-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

DOI:10.1080/10286020.2020.1729136

Reference yield: 21.0%

methanol (67-56-1) + sodium benzoate (532-32-1) + methanesulfonic acid (quinolin-4-yl)(5-vinyl-1-azabicyclo[2.2.2]oct-2-yl)methyl ester (560119-43-9) → benzoylcinchonine (14402-57-4,1260207-33-7) + (1S,4S,5R)-2-((S)-methoxy(quinolin-4-yl)methyl)-5-vinylquinuclidine + 3-methoxy-2-(quinolin-4-yl)-6-vinyl-1-azabicyclo[3.2.2]nonane + benzoic acid 2-(quinolin-4-yl)-6-vinyl-1-azabicyclo[3.2.2]non-3-yl-ester (560119-48-4)

Guidance literature:

for 84h; Heating;

DOI:10.1021/jo026890d

upstream raw materials:

benzoyl chloride

Cinchonin

methanol

sodium benzoate

Downstream raw materials:

benzoic acid

Cinchonin

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