methyl 2-amino-6-hydroxypyrimidine-4-carboxylate

Base Information

• Chemical Name: methyl 2-amino-6-hydroxypyrimidine-4-carboxylate
• CAS No.: 21615-64-5
• Molecular Formula: C6H7N3O3
• Molecular Weight: 169.1381
• Mol file: 21615-64-5.mol

Synonyms:methyl 2-amino-6-hydroxypyrimidine-4-carboxylate;2-amino-6-oxo-1,6-dihydro-pyrimidine-4-carboxylic acid methyl ester;

Chemical Property of methyl 2-amino-6-hydroxypyrimidine-4-carboxylate

Chemical Property:

• Vapor Pressure: 0.000353mmHg at 25°C
• Melting Point: 279-281 °C (decomp)
• Boiling Point: 318.8°Cat760mmHg
• PKA: 7.44±0.50(Predicted)
• Flash Point: 146.6°C
• PSA: 98.07000
• Density: 1.58g/cm³
• LogP: -0.28010

Purity/Quality:

99% ^*data from raw suppliers

Methyl2-amino-6-hydroxypyrimidine-4-carboxylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of methyl 2-amino-6-hydroxypyrimidine-4-carboxylate

There total 3 articles about methyl 2-amino-6-hydroxypyrimidine-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + guanidine nitrate (113-00-8) + diethyl oxaloacetate (108-56-5) → 2-Amino-6-hydroxy-pyrimidin-carbonsaeure-(4)-methylester (21615-64-5)

Guidance literature:

guanidine nitrate; diethyl oxaloacetate; With sodium hydroxide; In water; at 20 ℃; for 3.5h;

methanol; With sulfuric acid; for 18h; Reflux;

DOI:10.1016/j.bmc.2009.07.078

Reference yield:

→ 2-Amino-6-hydroxy-pyrimidin-carbonsaeure-(4)-methylester (21615-64-5)

Guidance literature:

2-Amino-6-hydroxy-pyrimidin-carbonsaeure-(4), Me., konz. H2SO4;

DOI:10.1021/jo01066a033

Reference yield:

→ Methyl 2-amino-6(1H)oxo-4-pyrimidin-carboxylat (21615-64-5)

Guidance literature:

Pyrimidin (IId);

DOI:10.1039/c29710000864

upstream raw materials:

methanol

guanidine nitrate

diethyl oxaloacetate

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