N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

Base Information

Chemical Name:N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide
CAS No.:1427407-32-6
Molecular Formula:C₂₀H₁₃Cl₂F₂NO₂
Molecular Weight:408.232
Hs Code.:

Synonyms:N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

Chemical Property:

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Technology Process of N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

There total 6 articles about N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 21.0%

: 1214382-15-6
C₁₃H₇ClF₂O

: 55285-43-3
2,6-dichloro-3-methoxyphenylamine

: 1427407-32-6
N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 20 ℃; for 2h;

Reference yield:

: 38902-87-3
3-nitro-2,4-dichlorophenol

: 1427407-32-6
N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / acetone / 0.5 h / 20 °C

1.2: 20 °C

2.1: palladium 10% on activated carbon; hydrogen / ethyl acetate

3.1: sodium hydride / tetrahydrofuran / 2 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; potassium carbonate; In tetrahydrofuran; ethyl acetate; acetone;

Reference yield:

: 1618-56-0
1,3-dichloro-4-methoxy-2-nitro-benzene

: 1427407-32-6
N-(2,6-dichloro-3-methoxy-phenyl)-2-fluoro-5-(3-fluorophenyl)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / ethyl acetate

2: sodium hydride / tetrahydrofuran / 2 h / 20 °C

With palladium 10% on activated carbon; hydrogen; sodium hydride; In tetrahydrofuran; ethyl acetate;