2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

Base Information

Chemical Name:2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene
CAS No.:1198166-47-0
Molecular Formula:C₂₇H₂₅F₆IO₄
Molecular Weight:654.388
Hs Code.:

Synonyms:2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

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Chemical Property of 2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

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Technology Process of 2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

There total 6 articles about 2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1198166-46-9
2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-propylphenoxy)aniline

: 1198166-47-0
2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

Guidance literature:: With toluene-4-sulfonic acid; potassium iodide; sodium nitrite; In water; acetonitrile; at 0 - 20 ℃;
DOI:10.1016/j.bmc.2016.05.048

Reference yield:

: 100-39-0
benzyl bromide

: 1198166-47-0
2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

3: acetic acid; iron / water / 4 h / 20 °C

4: potassium iodide; toluene-4-sulfonic acid; sodium nitrite / water; acetonitrile / 0 - 20 °C

With iron; potassium carbonate; toluene-4-sulfonic acid; acetic acid; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2016.05.048

Reference yield:

: 446-36-6
5-fluoro-2-nitrophenol

: 1198166-47-0
2-(benzyloxy)-4-(4-(1,1,1,3,3,3-hexafluoro-2-(methoxymethoxy)propan-2-yl)-2-n-propylphenoxy)-1-iodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1 h / 60 °C

2: potassium carbonate / N,N-dimethyl-formamide / 3 h / 80 °C

3: acetic acid; iron / water / 4 h / 20 °C

4: potassium iodide; toluene-4-sulfonic acid; sodium nitrite / water; acetonitrile / 0 - 20 °C

With iron; potassium carbonate; toluene-4-sulfonic acid; acetic acid; potassium iodide; sodium nitrite; In water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2016.05.048