methyldiphenylstibane

Base Information

• Chemical Name: methyldiphenylstibane
• CAS No.: 30982-88-8
• Molecular Formula: C₁₃H₁₃Sb
• Molecular Weight: 290.996
• Mol file: 30982-88-8.mol

Synonyms:methyldiphenylstibane

Chemical Property of methyldiphenylstibane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of methyldiphenylstibane

There total 23 articles about methyldiphenylstibane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

methylantimony diiodide (30982-87-7) → methyldiphenylstibane (30982-88-8)

Guidance literature:

With phenylmagnesium bromide; In tetrahydrofuran; by refluxing for 1 h;

Reference yield: 89.0%

methylantimony diiodide (30982-87-7) + phenylmagnesium bromide (100-58-3) → methyldiphenylstibane (30982-88-8)

Guidance literature:

With ammonium chloride; In tetrahydrofuran; diethyl ether; reflux, 1 h, aq. NH4Cl adding to the mixt.; distn. in a high vac.;

Reference yield: 60.0%

triphenylantimony (603-36-1) → methyldiphenylstibane (30982-88-8)

Guidance literature:

With sodium; ammonium chloride; In ammonia; ratio of Sb(C6H5)3 and sodium = 1:2, 6 h, with NH4Cl destroyd the C6H5Na, adding CH3Cl, evapn. of NH3, extraction with THF and benzene; distn.;

DOI:10.1016/S0022-328X(00)81607-1

upstream raw materials:

methylmagnesium bromide

tetraphenyldistibane

methyl iodide

diphenyl(trimethylsilyl)stibine

Downstream raw materials:

{(C₆H₅)(CH₃)Sb}2(CH₂)3

bis(methylphenylstibino)butane

(C₆H₅)(CH₃)Sb(i-C₃H₇)

Ag(Sb(C₆H₅)2CH₃)4⁽¹⁺⁾*BF₄^(1-)=[Ag(Sb(C₆H₅)2CH₃)4]BF₄