phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

Base Information

Chemical Name:phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate
CAS No.:1300090-39-4
Molecular Formula:C₂₃H₂₀IN₃O₄
Molecular Weight:529.334
Hs Code.:

Synonyms:phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

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Chemical Property of phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

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Technology Process of phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

There total 3 articles about phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1H-1,2λ⁵,3-benzotriazol-2-yl({[(phenylmethyl)oxy]carbonyl}amino)acetic acid

: 51073-69-9
(2-amino-5-iodophenyl)(phenyl)methanone

: 1300090-39-4
phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: (2-amino-5-iodophenyl)(phenyl)methanone; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 0 ℃; for 3h;

1H-1,2λ⁵,3-benzotriazol-2-yl({[(phenylmethyl)oxy]carbonyl}amino)acetic acid; With 4-methyl-morpholine; In tetrahydrofuran; at 0 ℃; for 1h;

With ammonia; at 0 ℃; for 1h;

Reference yield:

: 124676-19-3
2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine

: 51073-69-9
(2-amino-5-iodophenyl)(phenyl)methanone

: 1300090-39-4
phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: (2-amino-5-iodophenyl)(phenyl)methanone; With oxalyl dichloride; N,N-dimethyl-formamide; In tetrahydrofuran; at 0 ℃; for 3h;

2-(benzotriazol-1-yl)-N-(benzyloxycarbonyl)glycine; With 4-methyl-morpholine; In tetrahydrofuran; at 0 - 20 ℃;

With ammonia; In methanol; at 0 ℃; for 1h;

Reference yield:

: 2835-77-0
(2-aminophenyl)(phenyl)methanone

: 1300090-39-4
phenylmethyl (1-amino-2-{[4-iodo-2-(phenylcarbonyl)phenyl]amino}-2-oxoethyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: Iodine monochloride / dichloromethane / -70 - 20 °C

2.1: N,N-dimethyl-formamide; oxalyl dichloride / tetrahydrofuran / 3 h / 0 °C

2.2: 0 - 20 °C

2.3: 1 h / 0 °C

With oxalyl dichloride; Iodine monochloride; N,N-dimethyl-formamide; In tetrahydrofuran; dichloromethane;