10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Base Information

Chemical Name:10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde
CAS No.:1334037-46-5
Molecular Formula:C₃₂H₃₀N₂O₃
Molecular Weight:490.602
Hs Code.:

Synonyms:10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Suppliers and Price of 10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

There total 4 articles about 10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.6%

: 1334037-45-4
(6-phenoxazin-10-yl-hexyl)diphenylamine

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 1334037-46-5
10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Guidance literature:: (6-phenoxazin-10-yl-hexyl)diphenylamine; N,N-dimethyl-formamide; With trichlorophosphate; In 1,2-dichloro-ethane; at 0 - 90 ℃; for 5h; Inert atmosphere;

With water; sodium hydroxide; In 1,2-dichloro-ethane;
DOI:10.1021/jo201057b

Reference yield:

: 1027856-54-7
(6-bromohexyl)diphenylamine

: 1334037-46-5
10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

1.2: 3 h / 20 °C / Inert atmosphere

2.1: trichlorophosphate / 1,2-dichloro-ethane / 5 h / 0 - 90 °C / Inert atmosphere

With potassium hydroxide; trichlorophosphate; In dimethyl sulfoxide; 1,2-dichloro-ethane; 2.1: Vilsmeier formylation;
DOI:10.1021/jo201057b

Reference yield:

: 629-03-8
1 ,6-dibromohexane

: 1334037-46-5
10-{6-[(4-formylphenyl)phenylamino]hexyl}-10H-phenoxazine-3-carbaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / 1,2-dimethoxyethane / 0.5 h / 20 °C / Inert atmosphere

1.2: 2 h / 85 °C / Inert atmosphere

2.1: potassium hydroxide / dimethyl sulfoxide / 0.5 h / 20 °C / Inert atmosphere

2.2: 3 h / 20 °C / Inert atmosphere

3.1: trichlorophosphate / 1,2-dichloro-ethane / 5 h / 0 - 90 °C / Inert atmosphere

With sodium hydride; potassium hydroxide; trichlorophosphate; In 1,2-dimethoxyethane; dimethyl sulfoxide; 1,2-dichloro-ethane; 3.1: Vilsmeier formylation;
DOI:10.1021/jo201057b