N,N-dimethyl-1-(3-nitrophenyl)methanamine

Base Information

• Chemical Name: N,N-dimethyl-1-(3-nitrophenyl)methanamine
• CAS No.: 15184-95-9
• Molecular Formula: C9H12 N2 O2
• Molecular Weight: 180.206

Synonyms:Benzylamine,N,N-dimethyl-m-nitro- (6CI,7CI,8CI); N,N-Dimethyl-3-nitrobenzylamine;N,N-Dimethyl-N-(3-nitrobenzyl)amine; NSC 207807

Chemical Property of N,N-dimethyl-1-(3-nitrophenyl)methanamine

Chemical Property:

• Vapor Pressure: 0.0126mmHg at 25°C
• Boiling Point: 259.9°C at 760 mmHg
• Flash Point: 111°C
• Density: 1.141g/cm³

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-dimethyl-1-(3-nitrophenyl)methanamine

There total 14 articles about N,N-dimethyl-1-(3-nitrophenyl)methanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

N,N-dimethylammonium chloride (506-59-2) + 1-bromomethyl-3-nitrobenzene (3958-57-4) → N-(3-nitrophenylmethyl)dimethylamine (15184-95-9)

Guidance literature:

With triethylamine; In N-methyl-acetamide; water;

Reference yield: 66.0%

3-nitro-benzaldehyde (99-61-6) + dimethyl amine (124-40-3) → N-(3-nitrophenylmethyl)dimethylamine (15184-95-9)

Guidance literature:

3-nitro-benzaldehyde; dimethyl amine; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With sodium tris(acetoxy)borohydride; In tetrahydrofuran; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1021/acs.jmedchem.6b01018

Reference yield: 49.0%

dimethyl amine (124-40-3) + 1-bromomethyl-3-nitrobenzene (3958-57-4) → N-(3-nitrophenylmethyl)dimethylamine (15184-95-9)

Guidance literature:

In acetonitrile; at 80 ℃; for 4h;

DOI:10.1021/acs.jmedchem.7b00468

upstream raw materials:

N,N'-dimethylbenzylamine

formic acid

ethanol

hexamethylenetetramine

Downstream raw materials:

3-((dimethylamino)methyl)aniline

trimethyl-(3-trimethylammonio-benzyl)-ammonium; diiodide

C₁₈H₁₈N₃O₅⁽¹⁺⁾*Cl^(1-)

C₁₈H₁₇Cl₂N₂O₃⁽¹⁺⁾*Cl^(1-)

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