3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

Base Information

Chemical Name:3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle
CAS No.:60623-95-2
Molecular Formula:C₁₄H₂₂O₃Si
Molecular Weight:266.412
Hs Code.:

Synonyms:3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

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Chemical Property of 3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

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Technology Process of 3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

There total 10 articles about 3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 18295-66-4
1-ethoxy-1-(trimethylsiloxy)ethene

: 100-52-7
benzaldehyde

: 60623-95-2
3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

Guidance literature:: In toluene; at 23 ℃; for 2h; Inert atmosphere; Molecular sieve;
DOI:10.3987/COM-09-S(S)133

Reference yield: 85.0%

: 75-77-4
chloro-trimethyl-silane

: (η5.C5H5)(CO)3WO(C6H5)CHCH2CO(OC2H5)

: tricarbonylcyclopentadienyltungsten(II) chloride

: 60623-95-2
3-phenyl-3-<(trimethylsilyl)oxy>propanoate d'ethyle

Guidance literature:: In not given; at room temp., mixture of silyated and unsilyated organic aldol product after chromy. (47% yield); detected by NMR;