2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol

Base Information

Chemical Name:2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol
CAS No.:155791-51-8
Molecular Formula:C₁₈H₃₆OSn
Molecular Weight:387.193
Hs Code.:

Synonyms:2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol

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Technology Process of 2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol

There total 1 articles about 2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 100073-20-9
tri-n-butyl-(1-cyclohex-1-enyl)-stannane

: 930-68-7
cyclohexenone

: (1α,2β,6β)-1-(tributylstannyl)-7-oxabicyclo{4.1.0}heptan-2-ol

: 155791-51-8
2-(Tri-n-butylstannyl)-2-cyclohexen-1-ol

: 156666-06-7
2-(tri-n-butylstannyl)-2-cyclohexen-1-one

Guidance literature:: With titanium(IV) isopropylate; oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; Irradiation (UV/VIS); Sn-compd. and porphine in CH2Cl2 cooled to -20°C, a stream of O2 passed through the soln., irrdn. with two 250-W sodium lamps for 7.5 h, addn. of Ti(O-i-Pr)4, stirred at 0°C for 15 h, addn. of ether and H2O, stirred at 20°C for 2 h; filtered, dried (MgSO4), concd., flash chromy. (silica gel, petroleum ether/ether 4:1); elem. anal., ratio erythro:threo = >95:5;