4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile

Base Information

• Chemical Name: 4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile
• CAS No.: 950583-52-5
• Molecular Formula: C₂₁H₁₇NO₄S
• Molecular Weight: 379.436

Synonyms:4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile

Chemical Property of 4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile

Chemical Property:

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Technology Process of 4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile

There total 1 articles about 4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-di(4-methoxyphenyl)ethanone (120-44-5) + methyl 2-cyano-3,3-bis(methylsulfanyl)acrylate (3490-92-4) → 4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile (950583-52-5)

Guidance literature:

DOI:10.1016/j.tet.2007.07.050

Reference yield: 90.0%

4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile (950583-52-5) + methylamine (74-89-5) → C21H18N2O4 (1119194-71-6)

Guidance literature:

In methanol; Reflux;

DOI:10.1016/j.tetlet.2008.11.098

Reference yield: 86.0%

4-methylsulfanyl-2-oxo-5,6-bis(4-methoxyphenyl)-2H-pyran-3-carbonitrile (950583-52-5) + Methyl thioglycolate (2365-48-2) → 3-amino-6,7-bis-(4-methoxyphenyl)-4-oxo-4H-thieno[3,2-c]pyran-2-carboxylic acid methyl ester

Guidance literature:

With triethylamine; L-proline; In dimethyl sulfoxide; at 90 ℃;

DOI:10.1039/c4ra11337c

upstream raw materials:

1,4-di(4-methoxyphenyl)ethanone

methyl 2-cyano-3,3-bis(methylsulfanyl)acrylate

Downstream raw materials:

C₂₁H₁₈N₂O₄

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