methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate

Base Information

• Chemical Name: methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate
• CAS No.: 156205-15-1
• Molecular Formula: C₂₅H₂₄O₅
• Molecular Weight: 404.463

Synonyms:methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate

Chemical Property of methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate

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Technology Process of methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate

There total 1 articles about methyl 4-pentacyclo<4.2.0.0^2,5.0^3,8.0^4,7>octane-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

cubane-1,4-dicarboxylic acid dimethyl ester (29412-62-2) + 4-methoxyphenyl magnesium bromide (13139-86-1) → methyl 4-pentacyclo<4.2.0.02,5.03,8.04,7>octane-1-carboxylate (156205-15-1)

Guidance literature:

In tetrahydrofuran; for 2h; Heating;

DOI:10.1246/bcsj.67.462

Reference yield: 100.0%

formic acid (64-18-6) + methyl 4-pentacyclo<4.2.0.02,5.03,8.04,7>octane-1-carboxylate (156205-15-1) → methyl 1-formyloxy-9,9-bis(4-methoxyphenyl)pentacyclo<4.3.0.02,5.03,8.04,7>nonane-4-carboxylate (156204-90-9)

Guidance literature:

for 1h; Ambient temperature;

DOI:10.1246/bcsj.67.462

Reference yield: 69.0%

methanol (67-56-1) + methyl 4-pentacyclo<4.2.0.02,5.03,8.04,7>octane-1-carboxylate (156205-15-1) → methyl 1-methoxy-9,9-bis(4-methoxyphenyl)pentacyclo<4.3.0.02,5.03,8.04,7>nonane-4-carboxylate (156204-91-0)

Guidance literature:

With toluene-4-sulfonic acid; Ambient temperature;

DOI:10.1246/bcsj.67.462

upstream raw materials:

cubane-1,4-dicarboxylic acid dimethyl ester

4-methoxyphenyl magnesium bromide

Downstream raw materials:

methyl 1-methoxy-9,9-bis(4-methoxyphenyl)pentacyclo<4.3.0.0^2,5.0^3,8.0^4,7>nonane-4-carboxylate

methyl 1-formyloxy-9,9-bis(4-methoxyphenyl)pentacyclo<4.3.0.0^2,5.0^3,8.0^4,7>nonane-4-carboxylate

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