4-Methoxy-N-Methyl-benzenepropanaMine

Base Information

• Chemical Name: 4-Methoxy-N-Methyl-benzenepropanaMine
• CAS No.: 83986-67-8
• Molecular Formula: C₁₁H₁₇NO
• Molecular Weight: 179.262
• Mol file: 83986-67-8.mol

Synonyms:1-(methylamino)-3-(p-methoxyphenyl)propane

Chemical Property of 4-Methoxy-N-Methyl-benzenepropanaMine

Chemical Property:

Purity/Quality:

98%min ^*data from raw suppliers

4-Methoxy-N-methyl-benzenepropanamine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Methoxy-N-Methyl-benzenepropanaMine

There total 5 articles about 4-Methoxy-N-Methyl-benzenepropanaMine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Methoxystyrene (637-69-4,24936-44-5) + bis-(dimethylamino)methane (51-80-9) → 1-(dimethylamino)-3-(p-methoxyphenyl)-2-propene (37986-83-7) + 1-(methylamino)-3-(p-methoxyphenyl)propane (83986-67-8) + 1-(dimethylamino)-3-acetoxy-3-(p-methoxyphenyl)-2-propene (87462-08-6)

Guidance literature:

With phosphoric acid; In acetic acid; at 115 ℃; for 5h; Yield given. Yields of byproduct given;

DOI:10.1021/jo00172a018

Reference yield:

4-Methoxystyrene (637-69-4,24936-44-5) + dimethyl amine (124-40-3) → 2-(4-methoxyphenyl)-N-methylpropan-1-amine + 1-(methylamino)-3-(p-methoxyphenyl)propane (83986-67-8)

Guidance literature:

With C₃₁H₅₃N₅Ti; In toluene; at 140 ℃; for 96h; Overall yield = 24 %; Overall yield = 65 mg; Inert atmosphere; Sealed tube;

DOI:10.1002/anie.201708959

Reference yield:

3-(4-methoxyphenyl)propionitrile (22442-48-4) → 1-(methylamino)-3-(p-methoxyphenyl)propane (83986-67-8)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; methanol. ammonia / 100 °C / 51485.6 Torr / Hydrogenation

2: benzene / anschliessend mit Dimethylsulfat und Erwaermen des Reaktionsprodukts mit wss. Aethanol

With ammonia; nickel; benzene;

upstream raw materials:

4-Methoxystyrene

bis-(dimethylamino)methane

3-(4-methoxyphenyl)propionitrile

3-(4-methoxy-phenyl)propionamide

Downstream raw materials:

C₁₅H₁₉ClN₄O

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