(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

Base Information

Chemical Name:(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀
CAS No.:876941-95-6
Molecular Formula:C₆₆H₁₄₄Ge₂Si₁₄
Molecular Weight:1476.25
Hs Code.:

(((CH<sub>3</sub>)3Si)7C<sub>6</sub>H<sub>2</sub>(CH)2C)2Ge<sub>2</sub>C<sub>6</sub>H<sub>10</sub>

Synonyms:(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

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Chemical Property of (((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

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Technology Process of (((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

There total 2 articles about (((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 876941-91-2
1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermyne

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 876941-95-6
(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

Guidance literature:: In hexane; under Ar atm. to soln. Ge compound in hexane was added soln. 2,3-dimethyl-1,3-butadiene in hexane at room temp., mixt. was stirred for 24 h; soln. was evapd. in vac., residue was recrystd. from hexane at -40°C;
DOI:10.1021/ja057205y

Reference yield:

: 857444-41-8
(E)-1,2-dibromo-1,2-bis(2,6-bis[bis(trimethylsilyl)methyl]-4-[tris(trimethylsilyl)methyl]phenyl)digermene

: 876941-95-6
(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

Guidance literature:: Multi-step reaction with 2 steps

1: KC₈ / benzene

2: hexane

With KC₈; In hexane; benzene;
DOI:10.1021/ja057205y

Reference yield: 97.0%

: 67-56-1
methanol

: 876941-95-6
(((CH₃)3Si)7C₆H₂(CH)2C)2Ge₂C₆H₁₀

: 876941-98-9
(((CH₃)3Si)7C₆H₂(CH)2C)2GeC₆H₁₀GeH(CH₃O)

Guidance literature:: In tetrahydrofuran; methanol; under Ar atm. to soln. Ge compound in THF was added soln. excess MeOH, mixt. was stirred for 24 h; soln. was evapd. in vac., residue was purified by GPLC; elem. anal.;
DOI:10.1021/ja057205y