3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

Base Information

Chemical Name:3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester
CAS No.:813420-07-4
Molecular Formula:C₁₇H₁₈Cl₃NO₄
Molecular Weight:406.693
Hs Code.:

Synonyms:3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

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Chemical Property of 3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

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Technology Process of 3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

There total 3 articles about 3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19145-60-9
endo-benzoic acid 8-methyl-8-aza-bicyclo[3.2.1]oct-3-yl ester

: 17341-93-4
2,2,2-Trichloroethyl chloroformate

: 813420-07-4
3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

Guidance literature:: With potassium carbonate; In benzene; for 96h; Heating;
DOI:10.1002/jps.2600691134

Reference yield:

: 98-88-4
benzoyl chloride

: 813420-07-4
3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: TEA / toluene / 3 h / Heating

2: K₂CO₃ / toluene / 2.33 h / Heating

With TEA; potassium carbonate; In toluene;
DOI:10.1021/jm040814g

Reference yield:

: 98-88-4
benzoyl chloride

: 813420-07-4
3-benzoyloxy-8-azabicyclo[3.2.1 ]octane-8-carboxylic acid 2,2,2-trichloroethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C

2: toluene / 16 h / 20 - 100 °C

With potassium tert-butylate; In tetrahydrofuran; toluene;