diethyl 2-(4-chlorobenzoyl)malonate

Base Information

Chemical Name:diethyl 2-(4-chlorobenzoyl)malonate
CAS No.:24045-70-3
Molecular Formula:C₁₄H₁₅ClO₅
Molecular Weight:298.723
Hs Code.:

Synonyms:diethyl 2-(4-chlorobenzoyl)malonate

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Chemical Property of diethyl 2-(4-chlorobenzoyl)malonate

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Technology Process of diethyl 2-(4-chlorobenzoyl)malonate

There total 4 articles about diethyl 2-(4-chlorobenzoyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 122-01-0
4-chloro-benzoyl chloride

: 105-53-3
diethyl malonate

: 24045-70-3
diethyl 2-(4-chlorobenzoyl)malonate

Guidance literature:: With samarium(III) chloride; triethylamine; In toluene; at 20 ℃; for 2h;
DOI:10.1021/ol701961z

Reference yield: 71.0%

: 201230-82-2
carbon monoxide

: 1679-18-1
4-Chlorophenylboronic acid

: 105-53-3
diethyl malonate

: 24045-70-3
diethyl 2-(4-chlorobenzoyl)malonate

Guidance literature:: diethyl malonate; With lithium tert-butoxide; In toluene; at 20 ℃; for 1h; Autoclave;

carbon monoxide; 4-Chlorophenylboronic acid; With palladium(II) trifluoroacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; silver(l) oxide; In toluene; at 20 - 80 ℃; for 12h; under 3800.26 Torr; Autoclave;
DOI:10.1039/c4ob00568f