phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

Base Information

Chemical Name:phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate
CAS No.:1414575-99-7
Molecular Formula:C₂₁H₂₃N₃O₅
Molecular Weight:397.431
Hs Code.:

Synonyms:phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

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Technology Process of phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

There total 3 articles about phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1414575-97-5
3-((2,2-dimethyl-1,3-dioxan-5-yl)methoxy)-4-methyl-1-phenyl-1H-pyrazol-5-amine

: 1885-14-9
phenyl chloroformate

: 1414575-99-7
phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

Guidance literature:: With sodium hydroxide; In water; ethyl acetate; at 20 ℃; for 16h;

Reference yield:

: 934397-98-5
5-amino-4-methyl-1-phenyl-1H-pyrazol-3(2H)-one

: 1414575-99-7
phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C

2: sodium hydroxide / ethyl acetate; water / 16 h / 20 °C

With potassium carbonate; sodium hydroxide; In water; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 100-63-0
phenylhydrazine

: 1414575-99-7
phenyl (3-(3-hydroxy-2-(hydroxymethyl)propoxy)-4-methyl-1-phenyl-1H-pyrazol-5-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-dioxane / 17 h / 110 °C

2: potassium carbonate / N,N-dimethyl-formamide / 16 h / 50 °C

3: sodium hydroxide / ethyl acetate; water / 16 h / 20 °C

With potassium carbonate; sodium hydroxide; In 1,4-dioxane; water; ethyl acetate; N,N-dimethyl-formamide;