2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

Base Information

Chemical Name:2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate
CAS No.:748798-78-9
Molecular Formula:C₂₇H₂₉NO₆
Molecular Weight:463.53
Hs Code.:

Synonyms:2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

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Chemical Property of 2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

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Technology Process of 2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

There total 6 articles about 2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 541-41-3
chloroformic acid ethyl ester

: 748798-77-8
2-(2-hydroxyethyl)-N-[2-(3-benzyloxyphenoxy)ethyl]benzamide

: 748798-78-9
2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

Guidance literature:: With pyridine; In chloroform; at 20 ℃; for 0.5h;
DOI:10.1021/jm049720x

Reference yield:

: 3769-41-3
3-Benzyloxyphenol

: 748798-78-9
2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

Guidance literature:: Multi-step reaction with 4 steps

1: 67 percent / 16 h / 180 °C

2: 96 percent / aq. NaOH / ethanol / 36 h / Heating

3: 32 percent / NH₄Cl / 8 h / 120 °C

4: 86 percent / pyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; sodium hydroxide; ammonium chloride; In ethanol; chloroform;
DOI:10.1021/jm049720x

Reference yield:

: 100-39-0
benzyl bromide

: 748798-78-9
2-{2-[({2-[2-(benzyloxy)phenoxy]ethyl}amino)carbonyl]phenyl}ethyl ethyl carbonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: K₂CO₃ / acetone / 1 h / Heating

1.2: 70 percent / acetone; acetonitrile / 96 h / Heating

2.1: 67 percent / 16 h / 180 °C

3.1: 96 percent / aq. NaOH / ethanol / 36 h / Heating

4.1: 32 percent / NH₄Cl / 8 h / 120 °C

5.1: 86 percent / pyridine / CHCl₃ / 0.5 h / 20 °C

With pyridine; sodium hydroxide; potassium carbonate; ammonium chloride; In ethanol; chloroform; acetone;
DOI:10.1021/jm049720x