8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

Base Information

Chemical Name:8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide
CAS No.:1030596-41-8
Molecular Formula:C₁₉H₁₇N₃O₄
Molecular Weight:351.362
Hs Code.:

Synonyms:8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

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Chemical Property of 8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

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Technology Process of 8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

There total 3 articles about 8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 934611-83-3
8-hydroxyquinaldine-5-nitro-7-carboxylic acid

: 104-84-7
para-methylbenzylamine

: 1030596-41-8
8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

Guidance literature:: In dichloromethane; for 4h;
DOI:10.1016/j.bmc.2008.02.065

Reference yield:

: 23051-08-3
8-hydroxy-2-methylquinoline-7-carboxylic acid

: 1030596-41-8
8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; nitric acid / 2 h / 5 °C

2: carbodiimide derivative / dichloromethane / 4 h / Reflux

With sulfuric acid; nitric acid; In dichloromethane;
DOI:10.2174/1573406410666150807111703

Reference yield:

: 826-81-3
2-methyl-8-quinolinol

: 1030596-41-8
8-hydroxy-2-methyl-5-nitroquinoline-7-carboxylic acid-4-methylbenzylamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydroxide / toluene / 16 h / Reflux

2: sulfuric acid; nitric acid / 2 h / 5 °C

3: carbodiimide derivative / dichloromethane / 4 h / Reflux

With sulfuric acid; nitric acid; potassium hydroxide; In dichloromethane; toluene; 1: |Kolbe-Schmidt Synthesis;
DOI:10.2174/1573406410666150807111703