Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

Base Information

Chemical Name:Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester
CAS No.:162792-25-8
Molecular Formula:C₇₆H₁₀₉O₁₁P
Molecular Weight:1229.67
Hs Code.:

Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

Synonyms:Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

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Chemical Property of Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

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Technology Process of Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

There total 11 articles about Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 30334-71-5
1,2-dipalmitoyl-sn-glycerol

: 162792-24-7
Diisopropyl-phosphoramidous acid benzyl ester (1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyl ester

: 162792-25-8
Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: With 1H-tetrazole; In dichloromethane; acetonitrile; for 20h; Ambient temperature;
DOI:10.1016/S0040-4020(97)10003-5

Reference yield:

: 162792-21-4
(1R,2R,3R,4S,5R)-3,4,5-Tris-benzyloxy-2-methoxymethoxy-cyclohexanol

: 162792-25-8
Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 73 percent / NaH, Bu₄NI / dimethylformamide / Ambient temperature

2: 77 percent / conc. HCl / methanol / 2 h / Heating

3: 100 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 24 h / Ambient temperature

4: 60 percent / tetrazole / CH₂Cl₂; acetonitrile / 20 h / Ambient temperature

With 1H-tetrazole; hydrogenchloride; N,N-diisopropylamine tetrazolide; tetra-(n-butyl)ammonium iodide; sodium hydride; In methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(97)10003-5

Reference yield:

: 162792-23-6
1D-2,4,5,6-tetra-O-benzyl-3-deoxy-myo-inositol

: 162792-25-8
Hexadecanoic acid (R)-2-[benzyloxy-((1R,2R,3S,4R,6R)-2,3,4,6-tetrakis-benzyloxy-cyclohexyloxy)-phosphanyloxy]-1-hexadecanoyloxymethyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / diisopropylammonium tetrazolide / CH₂Cl₂ / 24 h / Ambient temperature

2: 60 percent / tetrazole / CH₂Cl₂; acetonitrile / 20 h / Ambient temperature

With 1H-tetrazole; N,N-diisopropylamine tetrazolide; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(97)10003-5