9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Base Information

Chemical Name:9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate
CAS No.:1609106-33-3
Molecular Formula:C₄₄H₅₁N₅O₉S
Molecular Weight:825.983
Hs Code.:

9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Synonyms:9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Suppliers and Price of 9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

There total 8 articles about 9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 206265-18-1
tert-butyl (4-sulfamoylbenzyl)carbamate

: 1609106-32-2
3-(2-{[N-(6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}hexanoyl)glycyl]amino}phenyl)propanoic acid

: 1609106-33-3
9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 3.5h;

Reference yield:

: 88574-06-5
6-{[(9H-fluoren-9-ylmethoxy)carbonyl]amino}hexanoic acid

: 1609106-33-3
9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 20 °C

2: sodium hydrogencarbonate / tetrahydrofuran; water; 1,2-dimethoxyethane / 16 h / 20 °C

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3.5 h / 20 °C

With dmap; sodium hydrogencarbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dicyclohexyl-carbodiimide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water;

Reference yield:

: 88939-75-7
methyl (2E)-3-(2-aminophenyl)propenoate

: 1609106-33-3
9H-fluoren-9-ylmethyl{6-[(2-{[2-(3-{[(4-{[(tert-butoxycarbonyl)amino]methyl}phenyl)sulfonyl]amino}-3-oxopropyl)phenyl]amino}-2-oxoethyl)amino]-6-oxohexyl}carbamate

Guidance literature:: Multi-step reaction with 6 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; dmap / N,N-dimethyl-formamide / 18 h / 20 - 50 °C

2: palladium on activated charcoal; hydrogen / methanol; ethyl acetate / 9 h / 20 °C / 1551.49 Torr

3: water; sodium hydroxide / tetrahydrofuran / 3 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C

5: sodium hydrogencarbonate / tetrahydrofuran; water; 1,2-dimethoxyethane / 16 h / 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap / dichloromethane / 3.5 h / 20 °C

With hydrogenchloride; dmap; palladium on activated charcoal; water; hydrogen; sodium hydrogencarbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; 1,2-dimethoxyethane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide;