D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

Base Information

Chemical Name:D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine
CAS No.:123004-75-1
Molecular Formula:C₂₉H₃₈N₂O₉
Molecular Weight:558.629
Hs Code.:

D-N-(benzyloxycarbonyl)-2-<4-<D-3-<(tert-butoxycarbonyl)amino>-3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

Synonyms:D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

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Technology Process of D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

There total 3 articles about D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110207-49-3
tert-butyl D-N-(tert-butoxycarbonyl)homoserinate

: 123004-75-1
D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / carbon tetrabromide, triphenylphosphine / CH₂Cl₂ / 2 h / Ambient temperature

2: 1.) potassium hydride / 1.) DMF, RT, 10 min, 2.) RT, 3 h

With carbon tetrabromide; potassium hydride; triphenylphosphine; In dichloromethane;
DOI:10.1021/ja00158a040

Reference yield:

: 77004-75-2
(3R)-4-tert-butoxy-3-[(tert-butoxycarbonyl)amino]-4-oxobutanoic acid

: 123004-75-1
D-N-(benzyloxycarbonyl)-2-<4--3-(tert-butoxycarbonyl)propoxy>phenyl>glycine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) triethylamine, ethyl chloroformate, 2.) sodium borohydride / 1.) THF, RT, 30 min, 2.) water, RT, 4 h

2: 91 percent / carbon tetrabromide, triphenylphosphine / CH₂Cl₂ / 2 h / Ambient temperature

3: 1.) potassium hydride / 1.) DMF, RT, 10 min, 2.) RT, 3 h

With sodium tetrahydroborate; carbon tetrabromide; chloroformic acid ethyl ester; potassium hydride; triethylamine; triphenylphosphine; In dichloromethane;
DOI:10.1021/ja00158a040