4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Base Information

Chemical Name:4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide
CAS No.:1450923-27-9
Molecular Formula:C₂₄H₂₂N₄O₅S₂
Molecular Weight:510.594
Hs Code.:

Synonyms:4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

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Chemical Property of 4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

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Technology Process of 4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

There total 7 articles about 4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1450923-21-3
4-amino-3-hydroxy-N-(4-methoxybenzyl)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

: 70-11-1
α-bromoacetophenone

: 1450923-27-9
4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: With caesium carbonate; In acetonitrile; for 2h;

Reference yield:

: 2369-13-3
3-fluoro-4-nitroaniline

: 1450923-27-9
4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; sodium nitrite / water / 0.5 h / 0 °C

1.2: 1 h / 25 °C

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

2.2: 0.25 h / -78 °C

3.1: sodium trimethylsilanolate / tetrahydrofuran / 0 °C

4.1: acetic acid; iron / tetrahydrofuran / 40 h / Sealed tube; Heating

5.1: caesium carbonate / acetonitrile / 2 h

With hydrogenchloride; sodium trimethylsilanolate; iron; caesium carbonate; acetic acid; lithium hexamethyldisilazane; sodium nitrite; In tetrahydrofuran; water; acetonitrile;

Reference yield:

: 1443376-74-6
N-(4-methoxybenzyl)-1,2,4-thiadiazol-5-amine

: 1450923-27-9
4-amino-N-(4-methoxybenzyl)-3-(2-oxo-2-phenylethoxy)-N-(1,2,4-thiadiazol-5-yl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

1.2: 0.25 h / -78 °C

2.1: sodium trimethylsilanolate / tetrahydrofuran / 0 °C

3.1: acetic acid; iron / tetrahydrofuran / 40 h / Sealed tube; Heating

4.1: caesium carbonate / acetonitrile / 2 h

With sodium trimethylsilanolate; iron; caesium carbonate; acetic acid; lithium hexamethyldisilazane; In tetrahydrofuran; acetonitrile;