N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

Base Information

Chemical Name:N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine
CAS No.:1569982-85-9
Molecular Formula:C₂₁H₂₄N₄O₂
Molecular Weight:364.447
Hs Code.:

Synonyms:N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

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Chemical Property of N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

Chemical Property:

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Technology Process of N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

There total 9 articles about N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

: 1569986-42-0
(3-chloromethyl-4-methoxy-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

: 124-40-3
dimethyl amine

: 1569982-85-9
N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

Guidance literature:: In ethanol; at 50 ℃; for 3h; Sealed tube;

Reference yield:

: 75634-03-6
4-chloro-6-(2-methoxy-phenyl)-pyrimidine

: 1569982-85-9
N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 4 steps

1: tert-butyl alcohol / 6 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

3: phosphorus trichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C

4: ethanol / 3 h / 50 °C / Sealed tube

With lithium aluminium tetrahydride; phosphorus trichloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; tert-butyl alcohol;

Reference yield:

: 1569986-04-4
(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

: 1569982-85-9
N-(3-((dimethylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2: phosphorus trichloride / N,N-dimethyl-formamide; dichloromethane / 0 - 20 °C

3: ethanol / 3 h / 50 °C / Sealed tube

With lithium aluminium tetrahydride; phosphorus trichloride; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;