C₂HF₃O₂*C₁₄H₁₉F₂NO₂

Base Information

Chemical Name:C₂HF₃O₂*C₁₄H₁₉F₂NO₂
CAS No.:1352133-79-9
Molecular Formula:C₂HF₃O₂*C₁₄H₁₉F₂NO₂
Molecular Weight:385.331
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>14</sub>H<sub>19</sub>F<sub>2</sub>NO<sub>2</sub>

Synonyms:C₂HF₃O₂*C₁₄H₁₉F₂NO₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂HF₃O₂*C₁₄H₁₉F₂NO₂

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Technology Process of C₂HF₃O₂*C₁₄H₁₉F₂NO₂

There total 9 articles about C₂HF₃O₂*C₁₄H₁₉F₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1352133-74-4
methyl (3S)-3-(tert-butoxycarbonylamino)-2,2-difluoro-5-methylhexanoate

: 1352133-79-9
C₂HF₃O₂*C₁₄H₁₉F₂NO₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium hydroxide / ethanol; water / 1 h / 20 °C

1.2: 0 °C / Cooling with ice

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

2.2: 12 h / 20 °C

3.1: dichloromethane / 1.5 h / 0 °C

With caesium carbonate; lithium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100340

Reference yield:

: 111060-65-2
(S)-2-(dibenzylamino)-4-methylpentanal

: 1352133-79-9
C₂HF₃O₂*C₁₄H₁₉F₂NO₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: hexane; water / 0.08 h / 20 °C

1.2: 2 h / 20 °C

2.1: hydrogenchloride / 12 h / 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 1.5 h / -78 °C / Inert atmosphere

3.2: 0.5 h / -78 - 20 °C / Inert atmosphere

4.1: diethylamino-sulfur trifluoride / dichloromethane / 6 h / 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C

6.1: lithium hydroxide / ethanol; water / 1 h / 20 °C

6.2: 0 °C / Cooling with ice

7.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

7.2: 12 h / 20 °C

8.1: dichloromethane / 1.5 h / 0 °C

With hydrogenchloride; oxalyl dichloride; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; caesium carbonate; dimethyl sulfoxide; lithium hydroxide; In methanol; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100340

Reference yield:

: 100-39-0
benzyl bromide

: 1352133-79-9
C₂HF₃O₂*C₁₄H₁₉F₂NO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 12 h / 20 °C

2.1: dichloromethane / 1.5 h / 0 °C

With caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.201100340