6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

Base Information

Chemical Name:6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate
CAS No.:1345475-50-4
Molecular Formula:C₃₃H₃₁F₅N₂O₁₀
Molecular Weight:710.609
Hs Code.:

Synonyms:6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

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Chemical Property of 6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

Chemical Property:

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Technology Process of 6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

There total 6 articles about 6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1345471-52-4
(2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)prop-2-enoic acid

: 25952-53-8
1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride

: 96715-61-6
6-hydroxyhexyl 3,5-dinitrobenzoate

: 1345475-50-4
6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

Guidance literature:: With dmap; In dichloromethane; ethyl acetate; toluene;

Reference yield:

: 1345471-42-2
2-[4-(4,4,4-trifluorobutoxy)phenyl]-5,6-dihydro-4H-1,3-dithiin-1-ium trifluoromethanesulfonate

: 1345475-50-4
6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

2: palladium diacetate / N,N-dimethyl-formamide

3: 1,4-dioxane; water

4: dmap / dichloromethane; toluene; ethyl acetate

With dmap; bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;

Reference yield:

: 921623-31-6
4-(4,4,4-trifluorobutoxy)benzoic acid

: 1345475-50-4
6-[((2E)-3-(4-{difluoro[4-(4,4,4-trifluorobutoxy)phenyl]methoxy}phenyl)-prop-2-enoyl)oxy]hexyl 3,5-dinitrobenzoate

Guidance literature:: Multi-step reaction with 5 steps

1: trifluorormethanesulfonic acid

2: triethylamine; bromine; sodium hydrogencarbonate / dichloromethane; toluene; ethyl acetate

3: palladium diacetate / N,N-dimethyl-formamide

4: 1,4-dioxane; water

5: dmap / dichloromethane; toluene; ethyl acetate

With dmap; trifluorormethanesulfonic acid; bromine; palladium diacetate; sodium hydrogencarbonate; triethylamine; In 1,4-dioxane; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; toluene;