3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

Base Information

Chemical Name:3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone
CAS No.:1071178-87-4
Molecular Formula:C₁₇H₃₂O₂Si
Molecular Weight:296.525
Hs Code.:

Synonyms:3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

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Chemical Property of 3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

Chemical Property:

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Technology Process of 3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

There total 5 articles about 3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1071179-31-1
3-(3-(tert-butyldimethylsilyloxy)propyl)-6-methylcyclohex-2-enone

: 74-88-4
methyl iodide

: 1071178-87-4
3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

Guidance literature:: 3-(3-(tert-butyldimethylsilyloxy)propyl)-6-methylcyclohex-2-enone; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;

methyl iodide; In tetrahydrofuran; hexane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1002/chem.200800930

Reference yield:

: 61589-86-4
3-(3-hydroxy-propyl)cyclohex-2-en-1-one

: 1071178-87-4
3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

2.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere

2.2: -78 °C / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01086c

Reference yield:

: 5323-87-5
3-Ethoxycyclohex-2-en-1-one

: 1071178-87-4
3-(3-(tert-butyldimethylsilanyloxy)propyl)-6,6-dimethylcyclohex-2-enone

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / -20 - 20 °C / Inert atmosphere

2.1: 1H-imidazole / N,N-dimethyl-formamide / Inert atmosphere

3.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere

3.2: -78 °C / Inert atmosphere

4.1: lithium diisopropyl amide / tetrahydrofuran / -78 °C / Inert atmosphere

4.2: -78 °C / Inert atmosphere

With 1H-imidazole; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1039/c0ob01086c