3-(phenylthio)propanal dimethyl acetal

Base Information

Chemical Name:3-(phenylthio)propanal dimethyl acetal
CAS No.:52072-17-0
Molecular Formula:C₁₁H₁₆O₂S
Molecular Weight:212.313
Hs Code.:

Synonyms:3-(phenylthio)propanal dimethyl acetal

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Chemical Property of 3-(phenylthio)propanal dimethyl acetal

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Technology Process of 3-(phenylthio)propanal dimethyl acetal

There total 9 articles about 3-(phenylthio)propanal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 27098-65-3
3-phenylsulfanyl-propionaldehyde

: 149-73-5
trimethyl orthoformate

: 52072-17-0
3-(phenylthio)propanal dimethyl acetal

Guidance literature:: With toluene-4-sulfonic acid; In methanol; water; at 50 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.04.096

Reference yield: 81.0%

: 67-56-1
methanol

: 81850-14-8
(E)-1-methoxy-3-(phenylthio)propene

: 52072-17-0
3-(phenylthio)propanal dimethyl acetal

Guidance literature:: With methanesulfonic acid; for 21h;
DOI:10.1021/jo00381a014

Reference yield: 71.0%

: 36255-44-4
3-bromopropanal dimethyl acetal

: 629-45-8
dibutyl disulfide

: 52072-17-0
3-(phenylthio)propanal dimethyl acetal

Guidance literature:: With sodium hydroxide; Aminoiminomethanesulfinic acid; cetyltrimethylammonium chloride; In tetrahydrofuran; water; for 4h; Heating;
DOI:10.1016/0022-328X(87)80095-5