2-nitro-phenylacetaldehyde diethyl acetal

Base Information

• Chemical Name: 2-nitro-phenylacetaldehyde diethyl acetal
• CAS No.: 91873-10-8
• Molecular Formula: C₁₂H₁₇NO₄
• Molecular Weight: 239.271
• Mol file: 91873-10-8.mol

Synonyms:2-nitro-phenylacetaldehyde diethyl acetal

Chemical Property of 2-nitro-phenylacetaldehyde diethyl acetal

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 2-nitro-phenylacetaldehyde diethyl acetal

There total 2 articles about 2-nitro-phenylacetaldehyde diethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

ethyl nitrite (109-95-5) + 2-nitrostyrene (579-71-5) → (2-nitrophenyl)acetaldehyde (1969-73-9) + 2-nitro-phenylacetaldehyde diethyl acetal (91873-10-8)

Guidance literature:

With oxygen; sodium tetrachloropalladate(II); In ethanol; for 24h; Ambient temperature;

Reference yield:

sodium ethanolate (141-52-6) + trimethyl((2-nitrophenyl)ethynyl)silane (75867-47-9) → 2-nitro-phenylacetaldehyde diethyl acetal (91873-10-8)

Guidance literature:

In ethanol; for 4h; Yield given; Heating;

Reference yield: 98.0%

2-nitro-phenylacetaldehyde diethyl acetal (91873-10-8) → 2-aminophenylacetaldehyde diethyl acetal (91873-11-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; Ambient temperature;

upstream raw materials:

ethyl nitrite

2-nitrostyrene

sodium ethanolate

trimethyl((2-nitrophenyl)ethynyl)silane

Downstream raw materials:

2-aminophenylacetaldehyde diethyl acetal

indole