2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol

Base Information

• Chemical Name: 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol
• CAS No.: 1009044-49-8
• Molecular Formula: C₅₂H₆₉N₁₁O₅
• Molecular Weight: 928.191
• Mol file: 1009044-49-8.mol

Synonyms:2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol

Chemical Property of 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol

There total 1 articles about 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.7%

2,6-bis[bis(6-pivalamide-2-pyridylmethyl)aminomethyl]-4-nitrophenol (1136010-65-5) → 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol (1009044-49-8)

Guidance literature:

With hydrogen; palladium on activated charcoal; In methanol; at 45 ℃; under 760.051 Torr;

DOI:10.1039/b711802c

Reference yield:

iron(II) triflate + methanol (67-56-1) + sodium benzoate (532-32-1) + 2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenol (1009044-49-8) → [diiron(II)(2,6-bis[bis(6-pivalamido-2-pyridylmethyl)amino-methyl]-4-aminophenoxo)(benzoate)2]CF3SO3*MeOH

Guidance literature:

With Et₃N; In methanol; dichloromethane; CH2Cl2-MeOH soln. of C52H69N11O5, PhCOONa, Fe(CF3SO3)2 and Et3N stirred for a few h in a glove box; elem. anal., detd. by XRD;

DOI:10.1039/b711802c

upstream raw materials:

2,6-bis[bis(6-pivalamide-2-pyridylmethyl)aminomethyl]-4-nitrophenol