(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

Base Information Edit

Chemical Name:(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene
CAS No.:1015697-68-3
Molecular Formula:C₁₉H₂₁NO₆
Molecular Weight:359.379
Hs Code.:
Mol file:1015697-68-3.mol

Synonyms:(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

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Chemical Property of (Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene Edit

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Technology Process of (Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

There total 5 articles about (Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 132390-61-5
4-ethoxy-3-nitrobenzaldehyde

: 61240-20-8
triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide

: 1015697-68-3
(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

Guidance literature:: triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide; With n-butyllithium; In tetrahydrofuran; hexane; at -15 ℃; for 1h;

4-ethoxy-3-nitrobenzaldehyde; In tetrahydrofuran; hexane; at -15 - 20 ℃; UV-irradiation;

Reference yield: 50.0%

: 109-72-8,29786-93-4
n-butyllithium

: 132390-61-5
4-ethoxy-3-nitrobenzaldehyde

: 61240-20-8
triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide

: 1015697-68-3
(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

: C₁₉H₂₁NO₆

Guidance literature:: n-butyllithium; triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide; In tetrahydrofuran; hexane; Cooling with ice; Inert atmosphere;

4-ethoxy-3-nitrobenzaldehyde; In tetrahydrofuran; hexane; at 20 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.cclet.2015.05.003

Reference yield: 50.0%

: 74-96-4
ethyl bromide

: 3011-34-5
4-hydroxy-3-nitrobenzaldehyde

: 61240-20-8
triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide

: 1015697-68-3
(Z)-5-(4-ethoxy-3-nitrostyryl)-1,2,3-trimethoxybenzene

: C₁₉H₂₁NO₆

Guidance literature:: ethyl bromide; 4-hydroxy-3-nitrobenzaldehyde;

triphenyl-(3,4,5-trimethoxybenzyl)phosphonium bromide; With n-butyllithium;
DOI:10.1021/acs.jafc.5b05119