ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

Base Information

Chemical Name:ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate
CAS No.:1080623-42-2
Molecular Formula:C₂₂H₂₄ClFN₂O₄S
Molecular Weight:466.961
Hs Code.:

Synonyms:ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

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Chemical Property of ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

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Technology Process of ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

There total 7 articles about ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-(3-chloro-4-fluorobenzyl)-3-(phenylsulfinyl)-5,6-dihydropyridin-2(1H)-on

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 1080623-42-2
ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

Guidance literature:: With lithium 2-methylpropan-2-olate; In tetrahydrofuran; at 0 - 15 ℃; for 1h; Large scale;

Reference yield:

: diphenylketimine glycine ethyl ester

: 1-(3-chloro-4-fluorobenzyl)-3-(phenylsulfinyl)-5,6-dihydropyridin-2(1H)-on

: 1080623-42-2
ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

Guidance literature:: diphenylketimine glycine ethyl ester; 1-(3-chloro-4-fluorobenzyl)-3-(phenylsulfinyl)-5,6-dihydropyridin-2(1H)-on; With lithium tert-butoxide; In tetrahydrofuran; at 0 ℃; for 0.333333h;

With hydrogenchloride; In tetrahydrofuran; water; at 20 ℃; for 0.333333h;

Reference yield:

: 1080623-41-1
1-(3-chloro-4-fluorobenzyl)-3-(phenylsulfinyl)piperidin-2-one

: 60085-74-7
N,N-diphenylglycine

: 1080623-42-2
ethyl 2-amino-2-(1-(3-chloro-4-fluorobenzyl)-2-oxo-3-(phenylsulfinyl)piperidin-4-yl)acetate

Guidance literature:: 1-(3-chloro-4-fluorobenzyl)-3-(phenylsulfinyl)piperidin-2-one; N,N-diphenylglycine; With lithium tert-butoxide; In tetrahydrofuran; at 0 - 15 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water; at 0 - 20 ℃;