methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid)

Base Information

• Chemical Name: methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid)
• CAS No.: 345913-74-8
• Molecular Formula: C₁₂H₁₃N₃O₅
• Molecular Weight: 279.252
• Mol file: 345913-74-8.mol

Synonyms:methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid)

Chemical Property of methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid)

There total 1 articles about methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

methanol (67-56-1) + ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate (119935-81-8) + methylamine (74-89-5) → quinoxaline-2,3-dione (15804-19-0,6287-20-3) + methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid) (345913-74-8) + dimethyl ester of o-phenylenebis(oxamic acid) (1420065-48-0) + N1,N1'-(1,2-phenylene)bis(N2-methyloxalamide) (188727-95-9)

Guidance literature:

In ethanol; at 65 ℃; for 0.5h;

DOI:10.1039/c2dt32259e

Reference yield:

methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid) (345913-74-8) → (tetraphenylphosphonium)2[Ni(II)(o-phenylene(N'-methyloxamidate)oxamate)] tetrahydrate

Guidance literature:

Multi-step reaction with 2 steps

1: methanol

2: water

In methanol; water;

DOI:10.1039/b502478a

upstream raw materials:

methanol

ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate

methylamine