ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate

Base Information

• Chemical Name: ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate
• CAS No.: 119935-81-8
• Molecular Formula: C₁₄H₁₆N₂O₆
• Molecular Weight: 308.291

Synonyms:ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate

Chemical Property of ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate

Chemical Property:

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Technology Process of ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate

There total 1 articles about ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Ethyl oxalyl chloride (4755-77-5) + 1,2-diamino-benzene (95-54-5) → ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate (119935-81-8)

Guidance literature:

In tetrahydrofuran; for 0.5h; Heating;

Reference yield: 93.0%

(S)-valinol (2026-48-4,473-75-6) + ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate (119935-81-8) → N-(1-hydroxymethyl-2-methyl-propyl)-N'-{2-[(1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-phenyl}-oxalamide (910116-95-9)

Guidance literature:

In toluene; for 72h; Heating;

DOI:10.1021/jo060767v

Reference yield: 89.0%

methanol (67-56-1) + ethyl 2-[(2-{[2-(ethyloxy)-2-oxoacetyl]amino}phenyl)amino]-2-oxoethanoate (119935-81-8) + methylamine (74-89-5) → quinoxaline-2,3-dione (15804-19-0,6287-20-3) + methyl ester of o-phenylene(N′-methyloxamide)(oxamic acid) (345913-74-8) + dimethyl ester of o-phenylenebis(oxamic acid) (1420065-48-0) + N1,N1'-(1,2-phenylene)bis(N2-methyloxalamide) (188727-95-9)

Guidance literature:

In ethanol; at 65 ℃; for 0.5h;

DOI:10.1039/c2dt32259e

upstream raw materials:

Ethyl oxalyl chloride

1,2-diamino-benzene

Downstream raw materials:

1,2-Phenylenedioxamoylbis(γ-aminobutyric acid)

N-[2-(Methylaminooxalyl-amino)-phenyl]-oxalamic acid

N¹,N^1'-(1,2-phenylene)bis(N²-methyloxalamide)

N-(1-hydroxymethyl-2-methyl-propyl)-N'-{2-[(1-hydroxymethyl-2-methyl-propylaminooxalyl)-amino]-phenyl}-oxalamide

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