Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide

Base Information

Chemical Name:Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide
CAS No.:29110-75-6
Molecular Formula:C13H14 N2 O2 S
Molecular Weight:262.332
Hs Code.:
DSSTox Substance ID:DTXSID20183364
Nikkaji Number:J788.029D
Wikidata:Q83054127
Pharos Ligand ID:PMTAW5UXW9AA
ChEMBL ID:CHEMBL1330954
Mol file:29110-75-6.mol

Synonyms:29110-75-6;4-methyl-N'-phenylbenzenesulfonohydrazide;Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide;Benzenesulfonic acid, 4-methyl-, 2-phenylhydrazide;p-Methylbenzenesulfonic acid 2-phenylhydrazide;BRN 0751176;AI3-04878;MLS000577482;N(sub 1)-Benzen-N(sub 2)-p-tolylsulfonhydrazine;N(sub 1)-Benzen-N(sub 2)-p-tolylsulfonhydrazine [French];SMR000185472;4-15-00-00253 (Beilstein Handbook Reference);tosylaminoaniline;4-methyl-N'-phenyl-benzenesulfonohydrazide;1-Phenyl-2-tosylhydrazine;4-Methylbenzenesulfonic acid, 2-phenylhydrazide;cid_207054;CHEMBL1330954;SCHEMBL11161395;BDBM81038;DTXSID20183364;HMS2454B23;AKOS000274973;AKOS024348808;NCGC00245745-01;LS-32025;4-methyl-N''-phenylbenzenesulfonohydrazide;4-methyl-N''-phenyl-benzenesulfonohydrazide;SR-01000205381;SR-01000205381-1

Suppliers and Price of Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:262.07759887
Heavy Atom Count:18
Complexity:337

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)NNC2=CC=CC=C2

Technology Process of Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide

There total 14 articles about Benzenesulfonic acid, p-methyl-, 2-phenylhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 100-63-0
phenylhydrazine

: 98-59-9
p-toluenesulfonyl chloride

: 29110-75-6
N'-tosyl phenylhydrazine

Guidance literature:: With pyridine; In tetrahydrofuran; at 5 - 20 ℃; for 2h;

Reference yield:

: 941-55-9
4-toluenesulfonyl azide

: 62-53-3
aniline

: 68-34-8
phenyl toluenesulfonamide

: 80-30-8
N-cyclohexyl-p-toluenesulfonamide

: 6380-08-1
N-(4-aminophenyl)-4-methylbenzenesulfonamide

: 3624-90-6
N-tosyl-1,2-diaminobenzene

: 70-55-3
toluene-4-sulfonamide

: 29110-75-6
N'-tosyl phenylhydrazine

Guidance literature:: In cyclohexane; for 1.5h; Mechanism; Quantum yield; Irradiation;
DOI:10.1021/jo00160a024

Reference yield:

: 106-45-6
para-thiocresol

: 29110-75-6
N'-tosyl phenylhydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; trichlorophosphate / water; acetonitrile / 25 °C

2: Amberlite IRA-400 OH^(1-)-form / water; acetonitrile / 0.07 h / 25 °C

With dihydrogen peroxide; trichlorophosphate; In water; acetonitrile;
DOI:10.1016/j.tet.2012.04.040