3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid

Base Information

Chemical Name:3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid
CAS No.:87364-84-9
Molecular Formula:C₁₂H₁₃NO₇
Molecular Weight:283.238
Hs Code.:
European Community (EC) Number:668-156-8

Synonyms:SCHEMBL5717625;AKOS024324324;3-(3,4-DIMETHOXY-6-NITROBENZOYL)PROPIONIC ACID

Suppliers and Price of 3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:6
Exact Mass:283.06920175
Heavy Atom Count:20
Complexity:379

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=C(C=C(C(=C1)C(=O)CCC(=O)O)[N+](=O)[O-])OC

Technology Process of 3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid

There total 4 articles about 3-(3,4-Dimethoxy-6-nitrobenzoyl)propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 5333-34-6
3-(3,4-dimethoxybenzoyl)propionic acid

: 87364-84-9
2-(4,5-dimethoxy-2-nitrobenzoyl)propionic acid

Guidance literature:: With sulfuric acid; nitric acid; In acetic acid; below 50 grad C;

Reference yield:

: 91-16-7
1,2-dimethoxybenzene

: 87364-84-9
2-(4,5-dimethoxy-2-nitrobenzoyl)propionic acid

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / chlorobenzene / 1.) below 2 deg C 2.) 0 deg C, 1/2 h 3.) rt., 1 h

2: 91.5 percent / 2 N NaOH / 0.17 h / Heating

3: 65 percent / conc. HNO₃, conc. H₂SO₄ / acetic acid / below 50 grad C

With sodium hydroxide; aluminium trichloride; sulfuric acid; nitric acid; In acetic acid; chlorobenzene;

Reference yield:

: 14563-40-7
methyl 4-(3,4-dimethoxyphenyl)-4-oxobutanoate

: 87364-84-9
2-(4,5-dimethoxy-2-nitrobenzoyl)propionic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 91.5 percent / 2 N NaOH / 0.17 h / Heating

2: 65 percent / conc. HNO₃, conc. H₂SO₄ / acetic acid / below 50 grad C

With sodium hydroxide; sulfuric acid; nitric acid; In acetic acid;