(bromomethyl)(triphenyl)stannane

Base Information

Chemical Name:(bromomethyl)(triphenyl)stannane
CAS No.:199446-13-4
Molecular Formula:C₁₉H₁₇BrSn
Molecular Weight:443.958
Hs Code.:

Synonyms:(bromomethyl)(triphenyl)stannane

Suppliers and Price of (bromomethyl)(triphenyl)stannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (bromomethyl)(triphenyl)stannane

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of (bromomethyl)(triphenyl)stannane

There total 3 articles about (bromomethyl)(triphenyl)stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 557-68-6
iodobromomethane

: 639-58-7
triphenyltin chloride

: 199446-13-4
(bromomethyl)(triphenyl)stannane

Guidance literature:: iodobromomethane; triphenyltin chloride; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere;

With methyl lithium lithium bromide complex; In tetrahydrofuran; diethyl ether; at -78 ℃; for 1h; chemoselective reaction; Inert atmosphere;
DOI:10.1039/c8cc04786c

Reference yield: 30.0%

: 7789-23-3
potassium fluoride

: 962-89-0
triphenyltin bromide

: 74-95-3
1,1-dibromomethane

: 199446-13-4
(bromomethyl)(triphenyl)stannane

: 379-52-2
triphenyltinfluoride

Guidance literature:: With Zn; cupric acetate monohydrate; In tetrahydrofuran; N2-atmosphere; addn. of Ph3SnBr to soln. of BrZnCH2Br (prepared from Zn,CH2Br2 and cupric acetate) at 40°C, stirring overnight at 40.deg ree.C; evapn., extn. (hexane:3% aq. HCl), sepn. of org. layer, washing (dilutedHCl), evapn., dissoln. (ether), addn. of aq. KF, stirring for 3 h, filt ration off of Ph3SnF, sepn. of org. layer, drying (Na2SO4), addn. of EtOH, evapn.; elem. anal.;
DOI:10.1021/om970537u

Reference yield:

: 639-58-7
triphenyltin chloride

: 74-95-3
1,1-dibromomethane

: 199446-13-4
(bromomethyl)(triphenyl)stannane

Guidance literature:: 1,1-dibromomethane; With copper diacetate; zinc; In tetrahydrofuran; at 40 ℃; Schlenk technique; Inert atmosphere;

triphenyltin chloride; In tetrahydrofuran; at 40 ℃; for 6h; Schlenk technique; Inert atmosphere;