Dextraset

Base Information

• Chemical Name: Dextraset
• CAS No.: 7388-44-5
• Molecular Formula: C7H14N2O4
• Molecular Weight: 190.199
• Hs Code.: 2934999090
• European Community (EC) Number: 230-970-2
• NSC Number: 643488,68795
• UNII: S6O9AIU3WG
• DSSTox Substance ID: DTXSID2064656
• Nikkaji Number: J68.149K
• Wikidata: Q81991744
• Mol file: 7388-44-5.mol

Synonyms:Dextraset;Dextraset UN;7388-44-5;Rhonite R 2;Dimethoxymethyluron;3,5-bis(methoxymethyl)-1,3,5-oxadiazinan-4-one;N,N'-Bis(methoxymethyl)uron;Bis(methoxymethyl)uron;4H-1,3,5-Oxadiazin-4-one, tetrahydro-3,5-bis(methoxymethyl)-;Bis(methoxymethyl)(oxydimethylene)urea;Tetrahydro-3,5-bis(methoxymethyl)-4H-1,3,5-oxadiazin-4-one;S6O9AIU3WG;EINECS 230-970-2;NSC 68795;NSC-68795;NSC643488;NSC-643488;AI3-09491;UNII-S6O9AIU3WG;SCHEMBL2616352;N,N'-DIMETHOXYMETHYLURON;DTXSID2064656;NSC68795;Tetrahydro-3,3,5-oxadiazin-4-one;AKOS040768176;3,5-Bis(methoxymethyl)tetrahydro-4H-1,3,5-oxadiazine-4-one;4H-1,5-Oxadiazin-4-one, tetrahydro-3,5-bis(methoxymethyl)-;Tetrahydro-3,5-bis(methoxymethyl)-1,3,5,4H-oxadiazin-4-one;3,5-BIS(METHOXYMETHYL)TETRAHYDRO-4H-1,3,5-OXADIAZIN-4-ONE

Chemical Property of Dextraset

Chemical Property:

• Vapor Pressure: 0.00151mmHg at 25°C
• Boiling Point: 295.6°C at 760 mmHg
• Flash Point: 132.6°C
• PSA: 51.24000
• Density: 1.159g/cm³
• LogP: -0.26080
• XLogP3: -0.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 4
• Exact Mass: 190.09535693
• Heavy Atom Count: 13
• Complexity: 160

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: COCN1COCN(C1=O)COC

Technology Process of Dextraset

There total 6 articles about Dextraset which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanol (67-56-1) + tetra(hydroxymethyl)urea (2787-01-1) → 3,5-bis(methoxymethyl)perhydro-1,3,5-oxadiazin-4-one (7388-44-5)

Guidance literature:

With hydrogenchloride; In water; at 20 ℃; for 12h;

DOI:10.1002/mrc.4044

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + bis-(N'-hydroxymethyl-ureidomethyl)-ether (1910-86-7) → 3,5-bis(methoxymethyl)perhydro-1,3,5-oxadiazin-4-one (7388-44-5)

Guidance literature:

With barium dihydroxide; anschliessendes Behandeln mit wss.-methanol. HCl;

DOI:10.1007/BF00899274

Reference yield:

methanol (67-56-1) + formaldehyd (50-00-0,30525-89-4,61233-19-0) + urea (57-13-6) → 3,5-bis(methoxymethyl)perhydro-1,3,5-oxadiazin-4-one (7388-44-5) + tris(methoxymethyl)urea (13822-64-5)

Guidance literature:

With hydrogenchloride; sodium hydroxide; Yield given. Multistep reaction; 1.) water, 95 degC, 30 min, pH 9.6; 2.) 0-5 degC, 10 min;

DOI:10.1246/bcsj.62.1930

upstream raw materials:

formaldehyd

bis-(N'-hydroxymethyl-ureidomethyl)-ether

urea

methanol

Downstream raw materials:

3,5-bis-(2-hydroxy-3,5-dimethyl-benzyl)-tetrahydro-[1,3,5]oxadiazin-4-one

hexa-P-phenyl-P,P'-(4-oxo-[1,3,5]oxadiazinane-3,5-diyldimethyl)-bis-phosphonium; dibromide

3-hydroxymethyl-1,3,5-oxadiazinan-4-on

1,3,5-oxadiazinan-4-on