5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine)

Base Information

• Chemical Name: 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine)
• CAS No.: 322641-60-1
• Molecular Formula: C₄₂H₁₃F₁₅GaN₅
• Molecular Weight: 942.298
• Mol file: 322641-60-1.mol

Synonyms:5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine)

Chemical Property of 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine)

There total 5 articles about 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.6%

pyridine (110-86-1) + gallium(III) trichloride + 5,10,15-tris(pentafluorophenyl)corrole (238402-21-6) → 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine) (322641-60-1)

Guidance literature:

for 2h; Inert atmosphere; Reflux;

DOI:10.1039/c5dt03104d

Reference yield: 86.0%

pyridine (110-86-1) + gallium(III) trichloride + 5,10,15-tris(2,3,4,5,6-pentafluorophenyl)corrole (238402-21-6) → 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine) (322641-60-1)

Guidance literature:

Inert atmosphere; Reflux;

DOI:10.1002/chem.201704457

Reference yield: 76.0%

pyridine (110-86-1) + 5,10,15-tris(pentafluorophenyl)corrole + Gallium trichloride (13450-90-3) → 5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(pyridine) (322641-60-1)

Guidance literature:

In pyridine; soln. of org. compd. in pyridine added in large excess of flame-dried GaCl3, refluxed for 1 h under Ar; solvent evapd., chromy., recrystd. from CH2Cl2/heptane;

upstream raw materials:

pyridine

Gallium trichloride

5,10,15-tris(2,3,4,5,6-pentafluorophenyl)corrole

5,10,15-tris(pentafluorophenyl)corrole

Downstream raw materials:

5,10,15-tris(pentafluorophenyl)corrolate-3-carbaldehyde gallium(III)

2,17-bis-formyl-5,10,15-tris-(pentafluorophenyl)corrolatogallium(III)(bis-pyridine)

[(5,10,15-tris(pentafluorophenyl)corrole)Ga(pyridine)2]

3,17-dinitro-5,10,15-tris-(pentafluorophenyl)corrolato gallium(III)(bis-pyridine)