C₁₅H₂₀N₂O₂

Base Information

Chemical Name:C₁₅H₂₀N₂O₂
CAS No.:1424403-33-7
Molecular Formula:C₁₅H₂₀N₂O₂
Molecular Weight:260.336
Hs Code.:

C<sub>15</sub>H<sub>20</sub>N<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₅H₂₀N₂O₂

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Chemical Property of C₁₅H₂₀N₂O₂

Chemical Property:

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Technology Process of C₁₅H₂₀N₂O₂

There total 8 articles about C₁₅H₂₀N₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 1424403-05-3
(R)-6-(benzyloxy)-2-methylhexanoic acid

: 1424403-33-7
C₁₅H₂₀N₂O₂

Guidance literature:: (R)-6-(benzyloxy)-2-methylhexanoic acid; With chloroformic acid ethyl ester; triethylamine; In tetrahydrofuran; at -15 ℃; for 0.25h;

diazomethane; In tetrahydrofuran; diethyl ether; at 0 ℃; for 12h;
DOI:10.1016/j.tet.2013.01.048

Reference yield:

: 71126-73-3
6-benzyloxyhexan-1-ol

: 1424403-33-7
C₁₅H₂₀N₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethyl sulfoxide; oxalyl dichloride / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 0.5 h / -78 - 0 °C / Inert atmosphere

2.1: sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 1 h / 20 °C

3.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 1 h / -20 °C

3.2: 2 h / -20 - 0 °C

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

4.2: 3 h / -78 °C / Inert atmosphere

5.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 - 20 °C / Cooling with ice

6.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.25 h / -15 °C

6.2: 12 h / 0 °C

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; oxalyl dichloride; dihydrogen peroxide; sodium hexamethyldisilazane; chloroformic acid ethyl ester; pivaloyl chloride; dimethyl sulfoxide; triethylamine; lithium hydroxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.01.048

Reference yield:

: 130892-97-6
6-benzyloxyhexanoic acid

: 1424403-33-7
C₁₅H₂₀N₂O₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: pivaloyl chloride; triethylamine / tetrahydrofuran / 1 h / -20 °C

1.2: 2 h / -20 - 0 °C

2.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 3 h / -78 °C / Inert atmosphere

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 - 20 °C / Cooling with ice

4.1: triethylamine; chloroformic acid ethyl ester / tetrahydrofuran / 0.25 h / -15 °C

4.2: 12 h / 0 °C

With dihydrogen peroxide; sodium hexamethyldisilazane; chloroformic acid ethyl ester; pivaloyl chloride; triethylamine; lithium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.tet.2013.01.048